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Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia

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2012
167.pdf (1.706Mb)
Authors
Holclajtner-Antunović, Ivanka
Bajuk-Bogdanovic, Danica
Bikić, Vesna
Marić-Stojanović, Milica
Article (Published version)
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Abstract
A selection of Byzantine table pottery (17 samples) dating from the period between the beginning of the 12th century and the first half of the 13th century, discovered at Branicevo in Serbia, were analysed by Fourier transform infrared, micro-Raman and scanning electron microscopy with energy dispersive spectroscopy and petrography analysis. The aim of the investigation was to determine the chemical and mineralogical composition of the body and of the glaze and thus to determine the production technology. Fourier transform infrared spectroscopy provided data for estimating the firing temperature and the basic mineralogical composition, and micro-Raman spectroscopy was applied to study and characterise both the glaze and the body of the analysed sherds. It was found that noncalcareous clays, characterised by a rich mineral assemblage, were fired at temperatures between 700 and 900?degrees C. Oxidizing atmosphere was applied in the production of the red colour pottery. The dark and grey ...coloured paste of one group of sherds was produced by firing organic matter-rich clays in a reducing environment. The main type of transparent glaze was identified as lead-rich, and two samples were alkalilime glazed.

Keywords:
Raman spectroscopy / polymerisation index / minerals identification / medieval pottery / glaze
Source:
Journal of Raman Spectroscopy, 2012, 43, 8, 1101-1110
Publisher:
  • Wiley, Hoboken
Funding / projects:
  • Urbanisation Processes and Development of Mediaeval Society (RS-177021)
  • Electroconducting and redox-active polymers and oligomers: synthesis, structure, properties and applications (RS-172043)

DOI: 10.1002/jrs.3129

ISSN: 0377-0486

WoS: 000307550100021

Scopus: 2-s2.0-84865190705
[ Google Scholar ]
11
10
URI
http://rai.ai.ac.rs/handle/123456789/170
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Археолошки институт / Institute of Archaeology
TY  - JOUR
AU  - Holclajtner-Antunović, Ivanka
AU  - Bajuk-Bogdanovic, Danica
AU  - Bikić, Vesna
AU  - Marić-Stojanović, Milica
PY  - 2012
UR  - http://rai.ai.ac.rs/handle/123456789/170
AB  - A selection of Byzantine table pottery (17 samples) dating from the period between the beginning of the 12th century and the first half of the 13th century, discovered at Branicevo in Serbia, were analysed by Fourier transform infrared, micro-Raman and scanning electron microscopy with energy dispersive spectroscopy and petrography analysis. The aim of the investigation was to determine the chemical and mineralogical composition of the body and of the glaze and thus to determine the production technology. Fourier transform infrared spectroscopy provided data for estimating the firing temperature and the basic mineralogical composition, and micro-Raman spectroscopy was applied to study and characterise both the glaze and the body of the analysed sherds. It was found that noncalcareous clays, characterised by a rich mineral assemblage, were fired at temperatures between 700 and 900?degrees C. Oxidizing atmosphere was applied in the production of the red colour pottery. The dark and grey coloured paste of one group of sherds was produced by firing organic matter-rich clays in a reducing environment. The main type of transparent glaze was identified as lead-rich, and two samples were alkalilime glazed.
PB  - Wiley, Hoboken
T2  - Journal of Raman Spectroscopy
T1  - Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia
EP  - 1110
IS  - 8
SP  - 1101
VL  - 43
DO  - 10.1002/jrs.3129
ER  - 
@article{
author = "Holclajtner-Antunović, Ivanka and Bajuk-Bogdanovic, Danica and Bikić, Vesna and Marić-Stojanović, Milica",
year = "2012",
abstract = "A selection of Byzantine table pottery (17 samples) dating from the period between the beginning of the 12th century and the first half of the 13th century, discovered at Branicevo in Serbia, were analysed by Fourier transform infrared, micro-Raman and scanning electron microscopy with energy dispersive spectroscopy and petrography analysis. The aim of the investigation was to determine the chemical and mineralogical composition of the body and of the glaze and thus to determine the production technology. Fourier transform infrared spectroscopy provided data for estimating the firing temperature and the basic mineralogical composition, and micro-Raman spectroscopy was applied to study and characterise both the glaze and the body of the analysed sherds. It was found that noncalcareous clays, characterised by a rich mineral assemblage, were fired at temperatures between 700 and 900?degrees C. Oxidizing atmosphere was applied in the production of the red colour pottery. The dark and grey coloured paste of one group of sherds was produced by firing organic matter-rich clays in a reducing environment. The main type of transparent glaze was identified as lead-rich, and two samples were alkalilime glazed.",
publisher = "Wiley, Hoboken",
journal = "Journal of Raman Spectroscopy",
title = "Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia",
pages = "1110-1101",
number = "8",
volume = "43",
doi = "10.1002/jrs.3129"
}
Holclajtner-Antunović, I., Bajuk-Bogdanovic, D., Bikić, V.,& Marić-Stojanović, M.. (2012). Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia. in Journal of Raman Spectroscopy
Wiley, Hoboken., 43(8), 1101-1110.
https://doi.org/10.1002/jrs.3129
Holclajtner-Antunović I, Bajuk-Bogdanovic D, Bikić V, Marić-Stojanović M. Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia. in Journal of Raman Spectroscopy. 2012;43(8):1101-1110.
doi:10.1002/jrs.3129 .
Holclajtner-Antunović, Ivanka, Bajuk-Bogdanovic, Danica, Bikić, Vesna, Marić-Stojanović, Milica, "Micro-Raman and infrared analysis of medieval pottery findings from Branicevo, Serbia" in Journal of Raman Spectroscopy, 43, no. 8 (2012):1101-1110,
https://doi.org/10.1002/jrs.3129 . .

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